Chemistry and Biochemistry

2013

December 2013

C.I. Rogers, J.B. Oxborrow, R.R. Anderson, L. Tsai, G.P. Nordin, A.T. Woolley,“Microfluidic valves made from polymerized polyethylene glycol diacrylate,” unpublished manuscript. Retrieved from ScienceDirect.

M. M. Konnick, S.M. Bischof, D.H. Ess, R.A. Periana, B.G. Hashiguchi, “Base accelerated generation of N2 and NH3 from an osmium nitride,” unpublished manuscript. Retrieved from ScienceDirect.

J. Kister, D.H. Ess, W.R. Roush, “Enantio- and Diastereoselective Synthesis of syn-β-Hydroxy-α-vinyl Carboxylic Esters via Reductive Aldol Reactions of Ethyl Allenecarboxylate with 10-TMS-9-Borabicyclo[3.3.2]decane and DFT Analysis of the Hydroboration Pathway,” Organic Letters, 2013, volume 15/issue 21, pp. 5436-5439.

Q. Xu, H. Gao, M. Yousufuddin, D.H. Ess, L. Kürti, “Aerobic, Transition-Metal-Free, Direct, and Regiospecific Mono-α-arylation of Ketones: Synthesis and Mechanism by DFT Calculations,” Journal of the American Chemical Society, 2013, volume 135, pp. 14048-14051.

J. R. Shelton, M. A. Peterson, “Efficient Synthesis of 5’-O-(N)-Carbamyl and Polycarbamyl Nucleosides,” Tetrahedron Letters, 2013, volume 54, pp. 6882-6885.

B.L. Barney, R.T. Daly, D.E. Austin, “A multistage image charge detector made from printed circuit boards,” Review of Scientific Instruments, 2013, volume 84, pp. 114101 (1-6).

S. Kumar, J. Xuan, M.L. Lee, H.D. Tolley, A.R. Hawkins, A.T. Woolley, “Thin-film microfabricated nanofluidic arrays for sizeselective protein fractionation,” Lab Chip, 2013, volume 13, pp. 4591-4598.

K. Liu, H.D. Tolley, J.S. Lawson, M.L. Lee, “Highly crosslinked polymeric monoliths with various C6 functional groups for reversed-phase capillary liquid chromatography of small molecules,” Journal of Chromatography A, 2013, volume 1321, pp. 80-87.

November 2013

B.M. Trost, D.J. Michaelis, M.I. Truica, “Dinuclear Zinc—ProPhenol-Catalyzed Enantioselective α-Hydroxyacetate Aldol Reaction with Activated Ester Equivalents”, Organic Letters, 2013, volume 15/issue 17, pp. 4516-4519.

B.M. Trost, D.J. Michaelis, S. Malhotra, “Total Synthesis of (–)-18-epi-Peloruside A: An Alkyne Linchpin Strategy”, Journal of Organic Letters, 2013, doi:10.1021/ ol4024997.

E.J. Song, J. Kang, G.R. You, G.J. Park, Y. Kim, S. Kim, C. Kim, R.G. Harrison, “A single molecule that acts as a fluorescence sensor for zinc and cadmium and a colorimetric sensor for cobalt †”, Dalton Transactions, 2013, volume 42, pp. 15514-15520.

N. N. Jarenwattananon, S. Glöggler, T. Otto, A. Melkonian, W. Morris, S. R. Burt, O. M. Yaghi, L.-S. Bouchard, “Thermal maps of gases in heterogeneous reactions”, Nature, 2013, volume 502/issue 7472, pp. 537-540.

R.D. Chirico, M. Frenkel, J.W. Magee, V. Diky, C.D, Muzny, A.F. Kazakov, K. Kroenlein, I. Abdulagatov, G.R. Hardin, W.E. Acree Jr., J.F. Brenneke, P.L. Brown, P.T. Cummings, T.W. de Loos, D.G. Friend, A.R.H. Goodwin, L.D. Hansen, W.M. Haynes, N. Koga, A. Mandelis, K.N. Marsh, P.M. Mathias, C. McCabe, J.P. O’Connell, A. Pádua, V. Rives, C. Schick, J.P.M. Trusler, S. Vyazovkin, R.D. Weir, J. Wu, “Improvement of Quality in Publication of Experimental Thermophysical Property Data: Challenges, Assessment Tools, Global Implementation, and Online Support”, Journal of Chemical & Engineering Data, 2013, volume 58, pp. 2699-2716.

D.V. Peryshkov, W.P. Forrest, R.R. Schrock, S.J. Smith, P. Muller, “B(C6F5)3 Activation of Oxo Tungsten Complexes That Are Relevant to Olefin Metathesis”, Organometallics, 2013, volume 32/issue 19, pp. 5256- 5259.

E.M. Townsend, S.M. Kilyanek, R.R. Schrock, P. Muller, S.J. Smith, A.H. Hoveyda, “High Oxidation State Molybdenum Imido Heteroatom-Substituted Alkylidene Complexes”, Organometallics, 2013, volume 32/issue 16, pp. 4612-4617.

J. Yuan, R.R. Schrock, L.C.H. Gerber, P. Muller, S.J. Smith, “Synthesis and ROMP Chemistry of Decafluoroterphenoxide Molybdenum Imido Alkylidene and Ethylene Complexes”, Organometallics, 2013, volume 32/issue 10, pp. 2983-2992.

H. Jeong, D.J. Kozera, R.R. Schrock, S.J. Smith, J. Zhang, N. Ren, M.A. Hillmyer, “ZSelective Ring-Opening Metathesis Polymerization of 3-Substituted Cyclooctenes by Monoaryloxide Pyrrolide Imido Alkylidene (MAP) Catalysts of Molybdenum and Tungsten”, Organometallics, 2013, volume 32/ issue 17, pp. 4843-4850.

P. Müller, F.R. Fronczek, S.J. Smith, T. Mako, M. Levine, “Two polymorphs of 1,8-dichloroanthracene”, Acta Crystallogr., Sect. C: Cryst. Struct. Commun., 2013, volume 69/ issue 2, pp. 199-203.

R.K. Watt, O.D. Petrucci, T. Smith, “Ferritin as a model for developing 3rd generation nano architecture organic/inorganic hybrid photo catalysts for energy conversion”, Catalysis Science & Technology, 2013, doi:10.1039/C3CY00536D.

October 2013

K. Liu, P. Aggarwal, J.S. Lawson, H.D. Tolley, M.L. Lee, “Organic monoliths for highperformance reversed-phase liquid chromatography”, Journal of Separation Science, 2013, volume 36/issue 17, pp. 2767-2781.

B.J. Hansen, R.J. Niemi, A.R. Hawkins, S.A. Lammert, D.E. Austin, “A Lithographically Patterned Discrete Planar Electrode Linear Ion Trap Mass Spectrometer”, Journal of Microelectromechanical Systems, 2013,volume 22/issue 4, pp. 876-883.

September 2013

U. Hintermair, S.W. Sheehan, A.R. Parent, D.H. Ess, D.T. Richens, P.H. Vaccaro, G.W. Brudvig, R.H. Crabtree, “Precursor Transformation during Molecular Oxidation Catalysis with Organometallic Iridium Complexes”, Journal of the American Chemical Society, 2013, volume 135/issue 29, pp. 10837-10851.

K.D. Reichl, D.H. Ess, A.T. Radosevich, “Catalyzing Pyramidal Inversion: Configurational Lability of P-Stereogenic Phosphines via Single Electron Oxidation”, Journal of the American Chemical Society, 2013, volume 135/issue 25, pp. 9354-9357.

D.B. Pardue, S.J. Gustafson, R.A. Periana, D.H. Ess, T.R. Cundari, “Computational study of carbon-hydrogen bond deprotonation by alkali metal superbases”, Computational and Theoretical Chemistry, 2013, volume 1019, pp. 85-93.

J.A. Contreras, A. Wang, A.L. Rockwood, H.D. Tolley, M.L. Lee, “Dynamic thermal gradient gas chromatography”, Journal of Chromatography A, 2013, volume 1302, pp. 143-151.

D. Devarajan, C.E. Doubleday, D.H. Ess, “Theory of Divalent Main Group H2 Activation: Electronics and Quasiclassical Trajectories”, Inorganic Chemistry, 2013, volume 52/issue 15, pp. 8820-8833.

T. Ghebreghiorgis, B.H. Kirk, A. Aponick, D.H. Ess, “Multiple Mechanisms in Pd(II)- Catalyzed SN2´ Reactions of Allylic Alcohols”, The Journal of Organic Chemistry, 2013, volume 78/issue 15, pp. 7664-7673.

A.A. Chagovetz, C. Quinn, N. Damarse, L.D. Hansen, A.M. Chagovetz, R.L. Jensen, “Differential Scanning Calorimetry of Gliomas: A New Tool in Brain Cancer Diagnostics?”, Neurosurgery, 2013, volume 73/ issue 2, pp. 289-295.

E.S. Johnson, K.R. Lindblom, A. Robeson, R.D. Stevens, O.R. Ilkayeva, C.B. Newgard, S. Kornbluth, J.L. Andersen, “Metabolomic Profiling Reveals a Role for Caspase-2 in Lipoapoptosis”, The Journal of Biological Chemistry, 2013, volume 288/issue 20, pp. 14463-14475.

August 2013

G.K. Lam, M. Hopoate-Sitake, C.D. Adair, V.M. Buckalew, D.D. Johnson, D.F. Lewis, C.J. Robinson, G.R. Saade, S.W. Graves, “Digoxn antibody fragment, antigen binding (Fab), treatment of preeclampsia in women with endogenous digitalis-like factor: a secondary analysis of the DEEP Trial”, American Journal of Obstetrics & Gynecology, 2013, volume 209, pp. 1-6.

A.C. Pearson, M.R. Linford, J.N. Harb, R.C. Davis, “Dual Patterning of a Poly(acrylic acid) Layer by Electron-Beam and Block Copolymer Lithographies”, Langmuir, 2013, volume 29, pp. 7433-7438.

K.D. Reichl, D.H. Ess, A.T. Radosevich, “Catalyzing Pyramidal Inversion: Configurational Lability of P-Stereogenic Phosphines via Single Electron Oxidation”, Journal of the American Chemical Society, 2013, volume 135, pp. 9354-9357.

A.D. Curtis, A.R. Calchera, M.C. AsplundJ.E. Patterson, “Observation of sub-surface phenyl rings in polystyrene with vibrationally resonant sum-frequency generation”, Vibrational Spectroscopy, 2013, volume 68, pp. 71-81.

D.S. Jensen, S.S. Kanyal, N. Madaan, J.M. Hancock, A.E. Dadson, M.A. Vail, R. Vanfleet, V. Shutthanandan, Z. Zhu, M.H. Engelhard, M.R. Linford, “Multi-instrument characterization of the surfaces and materials in microfabricated, carbon nanotube-templated thin layer chromatography plates. An analogy to ‘The Blind Men and the Elephant’”, Surface and Interface Analysis, 2013, volume 45, pp. 1273-1282.

July 2013

N. A. Demarse, M. C. Killian, L. D. Hansen, C. F. Quinn, “Determining Enzyme Kinetics via Isothermal Titration Calorimetry,” Chapter in Enzyme Engineering: Methods and Protocols, Methods in Molecular Biology; J.C. Samuelson, Ed.; Springer: New York, 2013, volume 978, pp. 21–30.

H. Gao, D. H. Ess, M. Yousufuddin, L. Kürti, “Transition-Metal-Free Direct Arylation: Synthesis of Halogenated 2-Amino-2’- hydroxy-1, 1’-biaryls and Mechanism by DFT Calculations,” Journal of the American Chemical Society, 2013, volume 135, pp. 7086–7089.

G. Q. Li, H. Gao, C. Keene, M. Devonas, D. H. Ess, L. Kürtis, “Organocatalytic ArylAryl Bond Formation: An Atroposelective [3,3]-Rearrangement Approach to BINAM Derivatives,” Journal of the American Chemical Society, 2013, volume 135, pp. 7414–7417.

B. M. Loertscher, Y. Zhang, S. L. Castle, “Exploration of an Epoxidation-Ring–Opening Strategy for the Synthesis of Iyconadin A and Discovery of an Unexpected Payne Rearrangement,” Beilstein Journal of Organic Chemistry, 2013, volume 9, pp. 1179–1184.

June 2013

D. E. Allred, E.C. Bard, R.C. Davis, D.P. Hansen, M.R. Linford, B.M. Lunt, M.O. Worthington, “Optical data storage media containing substantially inert low melting temperature data layer”, U.S. Patent No. 8,389,095, March 5, 2013.

D.S. Jensen, S.S. Kanyal, N. Madaan, A.J. Miles, R.C. Davis, R. Vanfleet, M.A. Vail, A.E. Dadson, M.R. Linford, “Ozone priming of patterned carbon nanotube forests for subsequent atomic layer deposition-like deposition of SiO2 for the preparation of microfabricated thin layer chromatography plates”, Journal of Vaccum Science and Technology B 31(3), May/Jun 2013 031803-1.

B.M. Loertscher, P.R. Young, P.R. Evans, S.L. Castle, “Diastereoselective synthesis of vicinal tertiary diols”, 2013, First Tier Journal, 2013, pp. 1930-1933.

May 2013

S.E. Kalman, A. Petit, T.B. Gunnoe, D.H. Ess, T.R. Cundari, M. Sabat, “Facile and Regioselective C-H Bond Activation of Aromatic Substrates by an Fe(II) Complex Involving a Spin-Forbidden Pathway”, Organometallics, 2013, volume 32/issue 6, pp. 1797-1806

J.H. Kim, I.H. Hwang, S.P. Jang, J. Kang, S. Kim, I.Noh, Y. Kim, C. Kim, R.G. Harrison, “Zinc Sensors with Lower Binding Affinities for Cellular Imaging”, Dalton Transactions, 2013, volume 42, pp. 5500-5507

P.N. Nge, C.I. Rogers, A.T. Woolley, “Advances in Microfluidic Materials, Functions, Integration, and Applications”, Chemical Reviews, 2013, volume 113/issue 4, pp. 2250-2583

D. Li, A.D. Rands, S. C. Losee, B.C. Holt, J.R. Williams, S.A. Lammert, R.A. Robison, H.D. Tolley, M.L. Lee, “Automated Thermochemolysis Reactor for Detection of Bacillus Anthracis Endospores by Gas Chromatography-Mass Spectrometry”, Analytica Chimica Acta, 2013, volume 775, pp. 67-74.

April 2013

J. L. Andersen, S. Kornbluth, “The Tangled Circuitry of Metabolism and Apoptosis”, Molecular Cell, 2013, volume 49/issue 3, pp. 399-410

J.A. Contreras, A.L. Rockwood, H.D. Tolley, M.L. Lee, “Peak Sweeping and Gating Using Thermal Gradient Gas Chromatography”, Journal of Chromatography A, 2013, volume 1278, pp. 160-165

A. Wang, H.D. Tolley, M.L. Lee, “Gas Chromatography Using Resistive Heating Technology”, Journal of Chromatography A, 2012, volume 1261, pp. 46-57

A.C. Pearson, S. Jamieson, M.R. Linford, B.M. Lunt, R.C. Davis, “Oxidation of Grapheme ‘Bow Tie’ Nanofuses for Permanent, Write-Once-Read-Many Data Storage Device”, Nanotechnology, 2013, volume 24/issue 13, pp. 1-7

R.K. Watt, “A Unified Model for Ferritin Iron Loading by the Catalytic Center: Implications for Controlling “Free Iron: during Oxidative Stress”, Chembiochem, 2013, volume 14/issue 4, pp. 415-419

Y. Geng, A.C. Pearson, E.P. Gates, B. Uprety, R.C. Davis, J.N. Harb, A.T. Woolley, “Electrically Conductive Gold- and CopperMetallized DNA Origami Nanostructures”, Langmuir, 2013, volume 29/issue 10, pp. 3482-3490

S.J. Ness, R.R. Anderson, W. Hu, D.C. Richards, J. Oxborrow, T. Gustafson, B. Tsai, S. Kim, B. Mazzeo, A.T. Woolley, G.P. Nordin, “Weak Adsorption-Induced Surface Stress for Streptavidin Binding to Biotin Tethered to Silicon Microcantilever Arrays”,Sensors Journal, IEEE, 2013, volume 13/issue 3, pp. 959-968.

D. N. Mortensen, D.V. Dearden, “Influence of Charge Repulsion on Binding Strengths: Experimental and Computational Characterization of Mixed Alkali Metal Complexes of Decamethylcucurbit[5]uril in the Gas Phase”, Chemical Communications, 2011, volume 47, pp. 6081-6083

J.P. Wright, M.S. Heywood, G.K. Thurston, P.B. Farnsworth, “The Effects of Added Hydrogen on a Helium Atomspheric-Pressure Plasma Jet Ambient Desorption/Ionization Source”, J. Am. Soc. Mass Spectrom. 2013, volume 24/issue 3, pp. 335-340

J.D. Kerby, R.T. Daly, D.E. Austin, “A Novel Particle Source Based on Electrospray Charging for Dust Accelerators and its Significance for Cosmic Dust Studies”, Earth Planets Space, 2013, volume 65/issue 3, pp. 157-165

V. Gupta, N. Madaan, D.S. Jensen, S.C. Kunzler, M.R. Linford, “Hydrogen Plasma Treatment of Silicon Dioxide for Improved Silane Deposition”, Langmuir, 2013, volume 29/issue 11, pp. 3604-3609